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Department Structure and Dynamics of Energy Materials

Program of the 5th X-ray school 25.-29. April, 10 a.m. - 4:30 p.m.

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5th X-ray school 25.-29. April 2022, 10 a.m. - 4:30 p.m.

MONDAY, 25.04.

GENERAL INTRODUCTION I:

  • Fundamentals of crystallography
  • Fundamentals of X-ray diffraction

  • Introduction into X-ray CoreLab
  • Pattern indexation by hand

TUESDAY, 26.04.

GENERAL INTRODUCTION II:

  • Elements of X-ray powder pattern, peak shapes, measuring strategies
  • Crystallographic databases: ICSD + ICDD-PDF

  • Applying Powder Cell to X-ray powder patterns

WEDNESDAY, 27.04.

HANDS-ON TRAINIG AND PATTERN ANALYSIS I:

  • Instrument introduction
  • Optics, detectors, sample carriers
  • Sample preparation and measuring parameters
  • Data conversion

  • Phase analysis of XRD powder pattern using Bruker EVA software

THURSDAY, 28.04.

HANDS-ON TRAINIG AND PATTERN ANALYSIS II:

  • Grazing incidence XRD
  • Non-ambient X-ray diffraction 
  • Automatic indexation
  • LeBail refinement using Fullprof suite

FRIDAY, 29.04.

HANDS-ON TRAINIG AND PATTERN ANALYSIS III:

  • Grazing incidence XRD 
  • Non-ambient X-ray diffraction 
  • Sequential refinements

  • Science talk
  • Closing
 

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