IRIS beamline at BESSY II extended with nanomicroscopy

Infrared image of the nucleolus in the nucleus of a fibroblast cell. The scale bar corresponds to 500 nanometres.

Infrared image of the nucleolus in the nucleus of a fibroblast cell. The scale bar corresponds to 500 nanometres. © HZB

The IRIS infrared beamline at the BESSY II storage ring now offers a fourth option for characterising materials, cells and even molecules on different length scales. The team has extended the IRIS beamline with an end station for nanospectroscopy and nanoimaging that enables spatial resolutions down to below 30 nanometres. The instrument is also available to external user groups. 

The infrared beamline IRIS at the BESSY II storage ring is the only infrared beamline in Germany that is also available to external user groups and is therefore in great demand. Dr Ulrich Schade, in charge of the beamline, and his team continue to develop the instruments to enable unique, state-of-the-art experimental techniques in IR spectroscopy. 

As part of a recent major upgrade to the beamline, the team, together with the Institute of Chemistry at Humboldt University Berlin, has built an additional infrared near-field microscope.

"With the nanoscope, we can resolve structures smaller than a thousandth of the diameter of a human hair and thus reach the innermost structures of biological systems, catalysts, polymers and quantum materials," says Dr Alexander Veber, who led this extension.

The new nanospectroscopy end station is based on a scanning optical microscope and enables imaging and spectroscopy with infrared light with a spatial resolution of more than 30 nm. To demonstrate the performance of the new end station, Veber analysed individual cellulose microfibrils and imaged cell structures. All end stations are available to national and international user groups. 

Funding information: Bundesministerium für Bildung und Forschung [grant No. project 05K19KH1 (SyMS)]; Germany's Excellence Strategy (grant No. EXC 2008-390540038 – UniSysCat).

arö


You might also be interested in

  • Small powerhouses for very special light
    Science Highlight
    27.06.2024
    Small powerhouses for very special light
    An international team presents the functional principle of a new source of synchrotron radiation in Nature Communications Physics. Steady-state microbunching (SSMB) allows to build efficient and powerful radiation sources for coherent UV radiation in the future. This is very attractive for applications in basic research as well in the semiconductor industry.
  • New Method for Absorption Correction to Improve Dental Fillings
    Science Highlight
    24.06.2024
    New Method for Absorption Correction to Improve Dental Fillings
    A research team led by Dr. Ioanna Mantouvalou has developed a method to more accurately depict the elemental distributions in dental materials than previously possible. The used confocal micro-X-ray fluorescence (micro-XRF) analysis provides three-dimensional elemental images that contain distortions. These distortions occur when X-rays pass through materials of different densities and compositions. By utilizing micro-CT data, which provides detailed 3D images of the material structure, and chemical information from X-ray absorption spectroscopy (XAS) experiments conducted in the laboratory (BLiX, TU Berlin) and at the synchrotron light source BESSY II, the researchers have improved the method.
  • MXenes for energy storage: Chemical imaging more than just surface deep
    Science Highlight
    17.06.2024
    MXenes for energy storage: Chemical imaging more than just surface deep
    A new method in spectromicroscopy significantly improves the study of chemical reactions at the nanoscale, both on surfaces and inside layered materials. Scanning X-ray microscopy (SXM) at MAXYMUS beamline of BESSY II enables the investigation of chemical species adsorbed on the top layer (surface) or intercalated within the MXene electrode (bulk) with high chemical sensitivity. The method was developed by a HZB team led by Dr. Tristan Petit. The scientists demonstrated among others first SXM on MXene flakes, a material used as electrode in lithium-ion batteries.