Dr. Raül Garcia Diez received poster award at the international synchrotron conference SRI 2018

Raül Garcia Diez is awarded the poster prize.

Raül Garcia Diez is awarded the poster prize. © SRI 2018

HZB researcher introduces unique operando characterization by soft X-ray spectroscopy

The HZB physicist Raül Garcia Diez has been awarded a poster prize at the international conference "Synchrotron Radiation Instrumentation 2018" (SRI 2018) in Taiwan. He presented how the HZB team intends to observe the reactions in electrocatalysts under "operando" conditions with soft X-rays from BESSY II.

“Operando" analysis is of vital importance for investigating catalytic processes in materials and getting insights into the chemical reaction. This enables researchers to understand the mechanisms that limit the performance and stability of electrocatalyst materials. However, "operando" characterization techniques for catalysts and liquid environments - especially for soft X-ray applications - have to been pushed beyond the current limits first.

"Operando" investigations in a wide energy range

Dr. Raül Garcia Diez is part of Dr.-Ing. Marcus Bär's young investigator research group, which is developing this experimental setup in the EMIL laboratory. This includes a compact X-ray spectrometer (HiTS: "High transmission soft x-ray emission spectrometer") and a flow-cell suited for electrochemistry. The X-ray optics designed for the HiTS spectrometer enable material investigations over an extremely wide energy range (from 50 to 2,000 eV).

"Our design sets new standards in the field of soft X-ray spectroscopy. I am happy that I could report at the conference about the progress made in developing the EMIL infrastructure for “operando” measurements. The poster award is a recognition of our work," says Raül Garcia Diez.

The International Conference on Synchrotron Radiation Instrumentation takes place every three years. With approximately 800 participants, it is the largest conference in this field; almost all synchrotron facilities in the world were represented at this year's conference with talks and posters.

(sz)


You might also be interested in

  • Small powerhouses for very special light
    Science Highlight
    27.06.2024
    Small powerhouses for very special light
    An international team presents the functional principle of a new source of synchrotron radiation in Nature Communications Physics. Steady-state microbunching (SSMB) allows to build efficient and powerful radiation sources for coherent UV radiation in the future. This is very attractive for applications in basic research as well in the semiconductor industry.
  • New Method for Absorption Correction to Improve Dental Fillings
    Science Highlight
    24.06.2024
    New Method for Absorption Correction to Improve Dental Fillings
    A research team led by Dr. Ioanna Mantouvalou has developed a method to more accurately depict the elemental distributions in dental materials than previously possible. The used confocal micro-X-ray fluorescence (micro-XRF) analysis provides three-dimensional elemental images that contain distortions. These distortions occur when X-rays pass through materials of different densities and compositions. By utilizing micro-CT data, which provides detailed 3D images of the material structure, and chemical information from X-ray absorption spectroscopy (XAS) experiments conducted in the laboratory (BLiX, TU Berlin) and at the synchrotron light source BESSY II, the researchers have improved the method.
  • MXenes for energy storage: Chemical imaging more than just surface deep
    Science Highlight
    17.06.2024
    MXenes for energy storage: Chemical imaging more than just surface deep
    A new method in spectromicroscopy significantly improves the study of chemical reactions at the nanoscale, both on surfaces and inside layered materials. Scanning X-ray microscopy (SXM) at MAXYMUS beamline of BESSY II enables the investigation of chemical species adsorbed on the top layer (surface) or intercalated within the MXene electrode (bulk) with high chemical sensitivity. The method was developed by a HZB team led by Dr. Tristan Petit. The scientists demonstrated among others first SXM on MXene flakes, a material used as electrode in lithium-ion batteries.