“VEKMAG” at BESSY II creates 3D magnetic fields in samples

A general view of the VEKMAG end-station. The vector magnet chamber (grey) is supported by a hexapod frame. Below the magnet  one can distinguish the detector chamber (green) and  in the forward direction the deposition chamber (dark grey) is displayed. The beam quality is monitored by a diagnostic chamber (yellow) positioned in front of the magnet chamber.

A general view of the VEKMAG end-station. The vector magnet chamber (grey) is supported by a hexapod frame. Below the magnet one can distinguish the detector chamber (green) and in the forward direction the deposition chamber (dark grey) is displayed. The beam quality is monitored by a diagnostic chamber (yellow) positioned in front of the magnet chamber. © Dr. Tino Noll

Together with HZB, teams from the Universität Regensburg, from the Freie Universität Berlin and from  the  Ruhr Universität Bochum have jointly set up a unique measurement station at BESSY II: a vector electromagnet consisting of three mutually perpendicular Helmholtz coils which enables  setting the local magnetic field at the sample position  to any orientation desired. The first measurements of magnetic materials, spin systems, and nanostructured magnetic samples are scheduled for early 2015.

“We have been working on this project for almost six years”, reports HZB physicist Dr. Florin Radu. He is coordinating the project with the three universities. The deposition chamber for the samples was designed at Freie Universität Berlin. Ruhr Universität Bochum built the detector chambers, and Universität Regensburg developed the concepts for  synchrotron beam-based ferromagnetic resonance experiments.

Rapid change of polarisation

In the meantime, Radu and his team ensured optimum characteristics of a new beamline for carrying out most sophisticated experiments: “We need an extremely stable beam, but we also want to be able to change the polarisation of the x-rays  very rapidly”, he explains. “For that reason, we developed a hexapod vacuum chamber with six moveable legs supporting a mirror. By changing the leg positions slightly, we can change the orientation of the first mirror and thereby the polarisation of the x-ray beam in just seconds – about one hundred times faster than before.” The tests show that this prototype arrangement improves the signal-to-noise ratio by a factor of more than ten.

Temperature between 1,6 K and 500 K

The new experimental station will not only facilitate many different kinds of studies, particularly in the soft X-ray region, but will also permit to carry out completely new studies that require  temperatures of 500 Kelvin right down to 1.6 Kelvin and magnetic fields as high as nine tesla. Simultaneously the  X-rays can penetrate the individual atoms and excite their outer electrons, enabling magnetic properties of the individual elements to be distinguished.

The main assets of the new VEKMAG end-station are experimental specifications that are unique in comparison with stations operating at other international facilities. In particular for element-specific and time-resolved measurements of ferromagnetic and paramagnetic resonances, as well as for spectroscopic and scattering experiments VEKMAG offers a unique sample environment. However, “VEKMAG will only attain its full potential,  once HZB has implemented a new innovative beam filling pattern  with variable pulse lengths at full photon intensities”, according to Radu, because “we can then investigate rapid spin dynamics  with sub-picosecond time resolutions.”

The VEKMAG project was funded by the German Federal Ministry for Education and Research (BMBF) through a grant of about four million Euros.

arö

  • Copy link

You might also be interested in

  • Langbeinites show talents as 3D quantum spin liquids
    Science Highlight
    23.08.2024
    Langbeinites show talents as 3D quantum spin liquids
    A 3D quantum spin liquid has been discovered in the vicinity of a member of the langbeinite family. The material's specific crystalline structure and the resulting magnetic interactions induce an unusual behaviour that can be traced back to an island of liquidity. An international team has made this discovery with experiments at the ISIS neutron source and theoretical modelling on a nickel-langbeinite sample.
  • Green hydrogen: ‘Artificial leaf’ becomes better under pressure
    Science Highlight
    31.07.2024
    Green hydrogen: ‘Artificial leaf’ becomes better under pressure
    Hydrogen can be produced via the electrolytic splitting of water. One option here is the use of photoelectrodes that convert sunlight into voltage for electrolysis in so called photoelectrochemical cells (PEC cells). A research team at HZB has now shown that the efficiency of PEC cells can be significantly increased under pressure.
  • Green hydrogen from direct seawater electrolysis- experts warn against hype
    News
    29.07.2024
    Green hydrogen from direct seawater electrolysis- experts warn against hype
    At first glance, the plan sounds compelling: invent and develop future electrolysers capable of producing hydrogen directly from unpurified seawater. But a closer look reveals that such direct seawater electrolysers would require years of high-end research. And what is more: DSE electrolyzers are not even necessary - a simple desalination process is sufficient to prepare seawater for conventional electrolyzers. In a commentary in Joule, international experts compare the costs and benefits of the different approaches and come to a clear recommendation.