nmTransmission NEXAFS
Saturation free and time resolved soft X-ray absorption on liquids and colloids for UE52-SGM and PM3
Methods
Time-resolved absorption, NEXAFS, EXAFS
Remote access
depends on experiment - please discuss with Instrument Scientist
| Station data | |
|---|---|
| Temperature range | room temperature |
| Pressure range | <10^-3 mbar |
| Detector | GaAsP diode or APD |
| Manipulators | - |
| Sample holder compatibility | - |
| Additional equipment | |
| Samples | Thin liquid films |
| Applicable at beamline(s) | |
| PM3 | 20 - 1900 eV |
| UE112_PGM-1 | 8 - 690 eV; for extreme values (<50 eV or >400 eV) contact the beamline crew |
| UE52_SGM | 100 - 1500 eV |
| U125-2_NIM | 6(4) - 40 eV |
| U49-2_PGM-1 | 85 - 1600 eV |
End station for time-resolved and steady-state soft x-ray absorption spectroscopy (XAS/NEXAFS/XANES/EXAFS) in transmission on liquid samples. The liquid sample is continiously refreshed in a flatjet system. The transmitted intensity of synchrotron radiation for ground state NEXAFS is measured with a gallium arsenide (GaAs) photodiode. Here, the average diode current is recorded as a measure of transmitted intensity. For static measurements the full filling pattern of BESSY II is used. For time resolved measurement a MHz laser is incoupled to the end station. For time resolved studies an avalanche photo diode (APD) is used to separate the "single bunch" in the hybrid filling pattern of BESSY II.
For details see: M. Fondell, S. Eckert, R. M. Jay, C. Weniger, W. Quevedo, J. Niskanen, B. Kennedy, F. Sorgenfrei, D. Shick, E. Giangrisostomi, R. Ovsyannikov, K. Adamzyk, N. Huse, P. Wernet, R. Mitzner, A. Föhlisch, "Time-resolved soft X-ray absorption spectroscopy in transmission mode onliquids at MHz repetition rates", Structural dynamicsRev. Sci. Instrum. 4, 054902 (2017).